Chapter 12 Laboratory: Chemical Kinetics 213
CUTIOA nS
Although the chemicals used in this laboratory are not
hazardous, it is good practice to wear splash goggles,
gloves, and protective clothing at all times.
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SBSTITUTIU oNS ANd modIfICATIoNS
- You may substitute any brand of fizzy tablets for the
Alka-Seltzer tablets. - If you don’t have Alka-Seltzer or similar tablets, you may
substitute small sticks of chalk or calcium carbonate
antacid tablets for the Alka-Seltzer tablets and cold and
warm dilute (~3 M) solutions of hydrochloric acid for the
water. If you do that, remember that hydrochloric acid is
corrosive and hazardous to handle.
POCEDURER
1.f you have not already done so, put on your splash I
goggles, gloves, and protective clothing.
- Weigh one of the tablets to 0.01 g and record its mass on
line A of Table 12-1. - Add about 100 mL of cold tap water to the foam cup.
(Use a foam cup rather than a beaker to keep the
mass of the reaction vessel and its contents under the
maximum capacity of your balance. If the combined
mass of the foam cup, Alka-Seltzer tablet, and 100 mL
of water is greater than the maximum capacity of your
balance, reduce the quantity of water accordingly.) - Weigh the foam cup and water and record the mass on
line B of Table 12-1. - Measure and record the temperature of the water on
line C of Table 12-1. - With the cup and water still on the balance, drop the
tablet into the cup. - Note the combined mass of the cup, water, and tablet
every five seconds and record each mass in Table 12-1.
(It may be helpful to have one person watching the
clock while another calls out the mass reading at each
5-second milestone.) - Continue recording the changing mass until you reach
one minute or until the reaction completes, as evidenced
by the cessation of bubbling. - When the reaction completes, record the final mass of
the cup, water, and tablet on line Q of Table 12-1.
Dispose of the spent solution and rinse out the cup.
Repeat steps 1 through 9, using hot tap water.
Repeat steps 1 through 9, using a mixture of half hot and
half cold tap water.
10.
11.
12.
dISpoSAL: All of the solutions from this laboratory can
be flushed down the drain with plenty of water.
FIGURE 12-1: Observing the mass change as the Alka-Seltzer
tablet reacts and carbon dioxide is evolved