Laboratory Methods of Inorganic Chemistry, 2nd English Ed. 1928

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INTRODUCTORY.

If an abundant air blast is available at a fairly steady pressure,
the most convenient and useful form of furnace is the gas


furnace, Fig. 1, made of fire clay supported by a casing of


sheet iron, into which the flame from a large blast lamp is


admitted through a hole near the bottom. In the absence of an


air blast, gasolene blowpipes, similar to those commonly used by
plumbers, serve almost as well as the gas blast lamps. The use


of charcoal furnaces is inexpensive and to be recommended even


at the present day. Such a furnace is shown in Fig. 2, one-tenth


its natural size. It is made of sheet iron and is about 250 cm.
high and 280 cm. wide. Larger furnaces may be built of fire


brick and connected with the chimney of the building. The


fire in such a furnace can be started with some glowing charcoal


which has been heated before the blast lamp; the furnace is then
fed with layers of charcoal and coke and finally with coke alone.


Fig. 2. Fig. 3.

For heating substances in glass or porcelain tubes, a flame

spreader placed on an ordinary Bunsen burner is used when only


short lengths are to be heated; for longer stretches a row burner,
as shown in Fig. 3, is employed, and to retain the heat a cover of
asbestos board can be supported just above the tube by means of
wires. The three supports for the tube can be protected by
wrapping wet asbestos pulp about them, pressing it firmly into

position and allowing it to dry. For higher temperatures over a


considerable length of tube a combustion furnace, such as is used
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