380 CHEMISTRY AND TECHNOLOGY OF EXPLOSIVES
water. For this purpose the installation described on p. 364 may be used, in which
a stream of molten TNT ejected under pressure impinges on two streams of cold
water at their point of contact (Fig. 84). Grains of TNT together with water fall
into a tank, and are conveyed to a centrifuge or to a vacuum filter. To remove
water the product is dried in a tunnel or tray drier at 50-60°C, i.e. at a
temperature below its melting point.
FIG. 93. Vessel for drying TNT. FIG. 94. Flaking of TNT.
The water and liquors from washing and sulphitation of TNT contain some
TNT both dissolved and suspended. For recovering the latter the water and wash
liquor are conveyed to “labyrinth” tanks equipped with baffles barring the passage
of suspended TNT, which settles at the bottom. In this way a certain amount of
lower grade TNT may be recovered.
British method
In the British method, crude, granulated TNT prior to sulphitation is washed
either batchwise -an operation not differing from the one described above - or
continuously.
The plant for continuous washing (Fig. 96) consists of a rectangular trough,
8 m long, 1.4 m wide and 1.3 m high. The trough is made of cast iron sections screwed