urbaf2

(Michael S) #1

420 CHEMISTRY AND TECHNOLOGY OF EXPLOSIVES


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m. p. 65°C

Bonecki and T. Urbanski [45] prepared the same substance, also from 2,4,6-tri-
nitrotoluene, but in a different way:

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The next steps were analogous to those mentioned earlier. High purity trinitrostyrene
was formed with m. p. 140°C.

LITERATURE


  1. K. A. KOBE and E. M. LANGWORTHY, Ind. Eng. Chem. 49, 801 (1957).

  2. A. G. GORST, Khimiya i tekhnologiya nitrosoyedinenii, Oborongiz, Moskva, 1940.

  3. B. D. KRAVCHINSKII, Spravochnik po proizvodstvu vzryvchatykh veshchestv (Edited by
    USHAKOV-LEBEDEV), Goskhimtekhizdat, Moskva-Leningrad, 1934.
    4.BUSSENIUS and EISENSTÜCK, Ann. 113, 151 (1860).
    5.F. K. BEILSTEIN and E. LUHMANN, Ann. 144, 274 (1864).
    6.E. NOELTING and S. FOREL, Ber. 18, 2670 (1885).
    7.J. J. BLANKSMA, Rec. trav. chim. 21, 256, 336 (1902); 25, 165 (1906); 27, 98 (1909).

  4. A. A. SOLONINA (1914-1918), see A. G. GORST, ref. [2].
    8a. O. G. FILIPOV (1914-1918), see A. G. GORST, ref. [2].

  5. M. MARQUEYROL and P. LORIETTE, (1915), see Desvergnes L., Chimie et Industrie 25, 507
    (1931); 26, 278, 527 (1932).

  6. N. JEPREMOV and A. TIKHOMROVA, Izv. Inst. Fiz.-Khim. Analiza 4, 65 (1928).

  7. J. M. BELL and J. P. SAWYER, Ind. Eng. Chem. 11, 1025 (1919).

  8. F. L. PRENTISS, Army Ordnance 4, 117, 184, 242 (1923).

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