136 Introduction to Renewable Biomaterials
53 Holtman KM, Chang HM, Kadla JF. An NMR comparison of the whole lignin from
milled wood, MWL, and REL dissolved by the DMSO/NMI procedure.J Wood
Chem Technol. 2007; 27 (3–4):179–200.
54 Hatcher PG. Dipolar-dephasing^13 C NMR studies of decomposed wood and
coalified xylem tissue: evidence for chemical structural changes associated with
defunctionalization of lignin structural units during coalification.Energy Fuels.
1988; 2 (1):48–58.
55 Park J, Meng J, Lim KH, Rojas OJ, Park S. Transformation of lignocellulosic
biomass during torrefaction.J Anal Appl Pyrolysis2013; 100 :199–206.
56 Holtman KM, Chang H-M, Kadla JF. Solution-state nuclear magnetic resonance
study of the similarities between milled wood lignin and cellulolytic enzyme lignin.
J Agric Food Chem. 2004; 52 (4):720–6.
57 Granata A, Argyropoulos DS. 2-Chloro-4, 4, 5, 5-tetramethyl-1, 3,
2-dioxaphospholane, a reagent for the accurate determination of the
uncondensed and condensed phenolic moieties in lignins.J Agric Food Chem.
1995; 43 (6):1538–44.
58 Ding S-Y, Himmel ME. The maize primary cell wall microfibril: a new model
derived from direct visualization.J Agric Food Chem. 2006; 54 (3):597–606.
59 Reis D, Vian B. Helicoidal pattern in secondary cell walls and possible role of
xylans in their construction.Comptes Rendus Biologies. 2004; 327 (9–10):785–90.
60 Balakshin M, Capanema E, Gracz H, Chang H-M, Jameel H. Quantification of
lignin–carbohydrate linkages with high-resolution NMR spectroscopy.Planta.
2011; 233 (6):1097–110.
61 Determination of protein content in biomass. Laboratory Analytical Procedure
(LAP) [Internet]. 2008.
62 Mosse J. Nitrogen-to-protein conversion factor for ten cereals and six legumes or
oilseeds. A reappraisal of its definition and determination. Variation according to
species and to seed protein content.J Agric Food Chem. 1990; 38 (1):18–24.
63 Fengel D, Wegener G.Wood: chemistry, ultrastructure, reactions.Walterde
Gruyter, Berlin; 1983.
64 Lupoi JS, Singh S, Simmons BA, Henry RJ. Assessment of lignocellulosic biomass
using analytical spectroscopy: an evolution to high-throughput techniques.Bioenerg
Res. 2014; 7 (1):1–23.
65 Lupoi JS, Singh S, Parthasarathi R, Simmons BA, Henry RJ. Recent innovations in
analytical methods for the qualitative and quantitative assessment of lignin.Renew
Sustainable Energy Rev. 2015; 49 :871–906.
66 Teeäär R, Serimaa R, Paakkarl T. Crystallinity of cellulose, as determined by
CP/MAS NMR and XRD methods.Polym Bull. 1987; 17 (3):231–7.
67 Newman R. Estimation of the lateral dimensions of cellulose crystallites using^13 C
NMR signal strengths.Solid State Nucl Magn Reson. 1999; 15 (1):21–9.
68 Oh S, Yoo D, Shin Y, Seo G. FTIR analysis of cellulose treated with sodium
hydroxide and carbon dioxide.Carbohydr Res. 2005; 340 (3):417–28.
69 Nelson M, O’Connor R. Relation of certain infrared bands to cellulose crystallinity
and crystal latticed type. Part I. Spectra of lattice types I, II, III and of amorphous
cellulose.J Appl Polym Sci. 1964; 8 (3):1311–24.
