AMPK Methods and Protocols

(Rick Simeone) #1

  1. The islets can be first placed in a fresh tube and washed by
    adding islet media into the tube, spinning during 2 min at
    1000 rpm, and afterward resuspended in fresh mouse islet
    media and placed in a 10 cm nontreated plate to skipsteps
    15 and 16. Nevertheless, we have found that, due to Histopa-
    que being carried with the islets, the islets sometimes don’t
    pellet adequately at the bottom of the 15 ml tube, in which case
    some of the islets are lost.

  2. This is to allow recovery from the collagenase digestion. Also,
    note that the mouse islet medium contains 11 mM glucose,
    which corresponds to the concentration found in plasma in
    fed mice.

  3. Isolation, manipulation, and maintenance of islets in vitro
    might lead to undesired AMPK activation. First, any contami-
    nation of fresh rodent islet preparations with exocrine tissue
    will markedly increase the measured AMPK activity. This is
    consistent with the higher levels of the enzyme in the exocrine
    tissue [24]. Secondly, very large islets have a hypoxic central
    core [35] and doubtless high AMPK activity. Maintenance of
    islets in culture for3 days before the assay was found to
    overcome this problem, probably by allowing time for contam-
    inating exocrine tissue and the hypoxic central cores of large
    islets, to necrose [36]. Another way of avoiding the problem is
    to either handpick the islets or filter the islets preparation on a
    100 μM cell strainer and only use the small ones for the assay.
    This is particularly important if overexpressing adenoviruses as
    they will not infect the core of large islets [37]. Nevertheless,
    this might not be possible when a high amount of islet material
    is required for downstream applications (such as measurement
    of activity with SAMS peptide assay). And thirdly, washing the
    islets in PBS before protein isolation can activate AMPK, this
    can be prevented by adding glucose in the PBS at the same
    concentration as in the culture conditions or by strictly using
    ice-cold PBS and keeping the samples on ice at all times.

  4. Human pancreatic islets are generally provided to our lab from
    several research groups around the world. Human islets are
    maintained in medium containing a low glucose concentration
    (5.5 mM glucose), which mimics blood glucose concentration
    after a meal. Human islet medium: RPMI without glucose (add
    glucose up to 5.5 mM), 10% (v/v) FBS, 1% (v/v) penicillin/
    streptomycin, and 2.5 mg/L amphotericin B.

  5. The potent and selective AMPK activators compound 13 and
    compound 991 were described previously [16, 17]. AMPK-
    DN and AMPK-CA virus [12] are available from our lab.

  6. The number of islets to be used will greatly vary depending on
    the sensitivity of the downstream application. We have used as


Manipulation and Measurement in Islets 427
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