96 ENVIRONMENTAL ENGINEERING
Filter
I
I Holes
6
Figure 5-7. The Gooch crucible, with filter, for determining suspended solids, and the
evaporating dish used for determining total solids.
EXAMPLE 5.3. Given the following data:
-Weight of a dish (such as shown in Fig. 5-7) = 48.6212 g,
-100mL of sample is placed in the dish and evaporated. New weight of dish and
--The dish is placed in a 550°C furnace, then cooled. New weight = 48.6300 g.
dry solids = 48.6432 g.
Find the total, volatile, and fixed solids.
(dish + dry solids) - (dish)
Total solids =
sample volume
48.6432 - 48.6212
100
= (220) 10-6 g/mL
= (220) 10-~ mg/d
= 220 mgL.
(dish + unburned solids) - (dish)
sample volume
Fixed solids =
48.6300 - 48.6212
100
= 88 mg/L
Total volatile solids = Total solids - Total fixed solids
= 220 - 88
= 132mgL