Laboratory Methods of Inorganic Chemistry, 2nd English Ed. 1928

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TRANSITION POINT. 37


When sulphur is heated in a test tube above 160° it becomes


dark and so viscous that the tube can be inverted without the


sulphur flowing out.



  1. Transition Point of Cuprous Mercurilodide Cu 2 [Hgl 4 ] and of


Sliver Mercuriiodide Ag 2 [HglJ.


First prepare mercuric iodide by precipitating a solution of


6.8 g. of mercuric chloride with a solution of 8.3 g. of potassium


iodide. Wash the precipitate once by decantation, and dissolve it


together with 8.3 g. of potassium iodide in 50 cc. of water. Mix


the filtered solution with another filtered, concentrated solution


containing 12 g. of blue vitriol, and pass sulphur dioxide into the


filtrate, in order to reduce the cupric salt. The sulphur dioxide


can be prepared from sodium sulphite and sulphuric acid (cf. foot-


note, page 71). A bright-red precipitate is produced of some-


what the appearance of mercuric iodide. Wash it thoroughly on


the suction filter and dry it in the hot closet. Yield, about 20 g.


Cuprous mercuriiodide is transformed at about 71° into a


black modification. The color change can be observed if a pinch


of the material is gently heated in a test tube over a free flame;


on cooling, the black color changes again to red. To determine


the transition temperature, a sample may be heated slowly in a


dry test tube which is immersed in a beaker of water containing


a thermometer that serves also as a stirrer. By means of several


repetitions, the transition temperature may be obtained in this


way with considerable accuracy.


The silver salt also of hydromercuriiodic acid, H 2 [Hg IJ, pos-


sesses a transition point between 40° and 50°, which is likewise


characterized by a change in color. Below this temperature the


salt is yellow; above, it is red.


Precipitate a few cubic centimeters of mercuric chloride solu-


tion with a solution of potassium iodide, and redissolve the pre-


cipitate in an excess of the precipitant. Then add a few drops of


silver nitrate solution and observe, without filtering, the change in


color of the precipitate on heating and cooling. This transition


point is less sharp than that of the copper salt.


64, 257 (1906). Hoffmann and Rothe, ibid. 55,113 (1906); Smith and Carson,
ibid. 63, 273 (1908). With respect to the influence of different forms of S on the
melting point, see Beckmann, Paul, and Liesch, Z. anorg. Chem, 103,189 (1917),

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