Scanning Electron Microscopy and X-Ray Microanalysis

255 17

Sample tilt: -15 degrees Sample tilt: 0 degrees Sample tilt: 15 degrees

Sample tilt: 30 degrees Sample tilt: 45 degrees Sample tilt: 60 degrees

Cu K-L3

1.31EO Emission

1.81 μm × 1.81 μm Cu K-L3

1.26EO Emission

1.81 μm × 1.81 μm Cu K-L3

1.27EO Emission

1.81 μm × 1.81 μm

Cu K-L3

1.35EO Emission

1.81 μm × 1.81 μm Cu K-L3

1.12EO Emission

1.81 μm × 1.81 μm Cu K-L3

1.3EO Emission

1.81 μm × 1.81 μm

. Fig. 17.34 Tilting a bulk sample

Sample tilt: -30 degrees Sample tilt: 0 degrees Sample tilt: 30 degrees

Zn K-L3

1.12EO Emission

2.19 μm × 2.19 μm Zn K-L3

1.05EO Emission

2.19 μm × 2.19 μm Zn K-L3

1.07EO Emission

2.19 μm × 2.19 μm

. Fig. 17.35 Tilting a spherical sample

17.2 · Simulation in DTSA-II