Scanning Electron Microscopy and X-Ray Microanalysis

512

29

{100}

{100}

{110}

{110}

{111}

{111}

Y

Y

Z

Z

X

X

. Fig. 29.25 Pole figures from the austenite (top) and the ferrite (bot-
tom). In the austenite pole figures the single orientation of the austen-
ite is shown by the arrangements of the poles that are shown. This was

also observed from. Fig. 29.23b. The complexity of the ferrite pole

figures is due to the many crystallographic variants of ferrite that form

from the single orientation of austenite

ab

. Fig. 29.26 A thin sample made for TKD of the fine two phase regions
in the Gibeon meteorite. The sample was prepared with conventional FIB
followed by low voltage ion FIB milling at 5 kV. a Secondary electron SEM

image of the thinned sample. b Scanning transmission electron image of

the sample at 30 kV

Chapter 29 · Characterizing Crystalline Materials in the SEM