Nature - USA (2020-08-20)

386 | Nature | Vol 584 | 20 August 2020 Article Mishima, O. & Stanley, H. E. The relationship between liquid, supercooled a ...

Data availability The data that support the findings of this study are available from the corresponding author upon request. Sou ...

Article Extended Data Fig. 1 | Density discontinuity at 740 K. a, Raw datasets of isothermal X-ray absorption profiles I/I 0 (wh ...

Extended Data Fig. 2 | Structure factors. Structure factors (S(Q)) of liquid sulfur collected on decompression along the isother ...

Article Extended Data Fig. 3 | Isothermal density discontinuity. Density of liquid sulfur as a function of temperature along iso ...

Extended Data Fig. 4 | LLCP in sulfur. a, b, X-ray absorption profiles I/I 0 in the horizontal (a) and vertical (b) directions i ...

Nature | Vol 584 | 20 August 2020 | 387 Article Additive manufacturing of silica aerogels Shanyu Zhao1,9 ✉, Gilberto Siqueira2,9 ...

388 | Nature | Vol 584 | 20 August 2020 Article during the sol–gel transition (Extended Data Fig. 3a). The ink has a shelf life ...

Nature | Vol 584 | 20 August 2020 | 389 the silica sol. These denser grains (Fig. 2f–i) form an interlocked particle packing wit ...

390 | Nature | Vol 584 | 20 August 2020 Article network of linked secondary silica particles and high mesoporosity (Fig. 2i). Th ...

Nature | Vol 584 | 20 August 2020 | 391 smartphones and optical devices. To illustrate the utility of silica aero- gel in therma ...

392 | Nature | Vol 584 | 20 August 2020 Article aerogel market in industrial and building insulation. In addition, the ease with ...

Methods Ink composition and preparation Polyethoxydisiloxane (PEDS) precursor^34. 173 ml Dynasylan 40 (ethyl silicate with an Si ...

Article brighter. There are also distinct bright areas, probably related to MnO 2 aggregations. The size of these MnO 2 -enriche ...

Imaging and videography Images and videos were taken with a digital SLR camera (Canon, EOS 100D) equipped with a high-performanc ...

Article Extended Data Fig. 1 | Photographs and hydrophobicity of 3D-printed silica aerogel objects. a–c, Photographs of the 3D-p ...

Extended Data Fig. 2 | Rheology of silica aerogel inks. a–d, Apparent viscosity as a function of applied shear rate (a, c), and ...

Article Extended Data Fig. 3 | Solidification and printing performance. a, The evolution of solidification of the silica aerogel ...

Extended Data Fig. 4 | X-ray tomography image analysis. a, Histogram of grey values with deconvoluted peaks of aerogel particles ...

Article Extended Data Fig. 5 | Spectroscopic data. a, b,^1 H–^29 Si (a) and^1 H–^13 C (b) cross-polarization magic-angle spinnin ...