Scanning Electron Microscopy and X-Ray Microanalysis

349 21 Si K-M3 Ti K-L3 2 mm SiK Si K-M3 1.21E-3 EmissionE8.95E-3 mission 5.09 mm x 5.09 mm Ti K-L3 5.09 mm x 5.09 mm TiKa a Mont ...

350 21 21.4 Pathological Electron Scattering Can Produce “Trace” Contributions to EDS Spectra 21.4.1 Instrumental Sources of Tra ...

351 21 entrance window or other hardware. However, the reality of the EDS measurement is likely to be quite different from this ...

352 21 10 mm 12 mm 14 mm 0102030405060708090100 16 mm 18 mm 20 mm 1 mm 0 200 400 600 800 1000 1200 810121416182022 Working dista ...

353 21 21.4.2 Assessing Remote Excitation Sources in an SEM-EDS System Remote excitation of X-rays can be assessed by measuring ...

354 21 Photon energy (keV) 0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 . Fig. 21.14 Sequence of measurements for determini ...

355 21 EDS detector window Collimator & electron trap Final lens Chamber wall BSE Aperture scattering Conventional SEM, path ...

356 21 Co unts Ag 0.0 2.0 4.0 6.0 8.0 Photon energy (keV) 10.0 12.0 14.0 16.0 18.0 20 Ti = 0.000005 Ta E 0 = 20 keV 8% Deadtime ...

357 21 21.5 Summary High count EDS spectra can be used to achieve limits of detection approaching a mass concentration of CDL = ...

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360 22 22.1 What Constitutes “Low” Beam Energy X-Ray Microanalysis? The incident beam energy, E 0 , is the parameter that deter- ...

361 22 Photon energy (keV) Photon energy (keV) Si_5keV Si_4keV Si_3keV Si_2.8keV Si_2.6keV Si_2.4keV Si_2.2keV Si_2.0keV Si_1.9k ...

362 22 Elemental measurement strategy for conventional beam energy analysis H He Li Be BCNOFNe Na Mg Al Si PSCl Ar K Ca Sc Ti VC ...

363 22 H He Li Be BCNOFNe Na Mg Al Si PSCl Ar KCaScTiVCr Mn Fe Co Ni Cu Zn Ga Ge As Se Br Kr Rb Sr YZrNbMoTcRuRhPdAgCdInSnSbTeIX ...

364 22 22.1.1 Characteristic X-ray Peak Selection Strategy for Analysis “Conventional” electron-excited X-ray microanalysis is t ...

365 22 creates the situation shown in. Fig. 22.5. At 5  keV, only one shell is available for all elements except Ca, Cd, In, and ...

366 22 Au, while at E 0 = 2.5 keV, the range for Na collapses to 0.12 μm (120 nm) in a C matrix to 0.02 μm (20 nm) in Au. 22.2.2 ...

367 22 (nitrides), and. Table 22.4 (oxides) (Newbury and Ritchie 2015 ). Examples of EDS spectra and the residual spectrum after ...

368 22 Photon energy (keV) Counts E 0 = 5 keV CrB 2 Fitting residual 35000 30000 25000 20000 15000 10000 5000 0 0.000.05 0.10 0. ...

369 22 Counts 80000 60000 40000 20000 0 0.00 0.10 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 Photon energy (keV) E 0 = 5 keV F ...