Scanning Electron Microscopy and X-Ray Microanalysis
307 19 φ(ρz) distribution. Once the X-ray-induced φ(ρz) generated distribution is determined, the absorption of the outgoing X-r ...
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20.6 Beam-Sensitive Specimens 20.6.1 Alkali Element Migration – 331 20.6.2 Materials Subject to Mass Loss During Electron Bombar ...
311 20 This chapter discusses the procedure used to perform a rig- orous quantitative elemental microanalysis by SEM/EDS followi ...
312 20 energy, E 0. The energy span is given by the channel width multiplied by the number of channels. With a 5-eV chan- nel wi ...
313 20 FWHM or more, depending on the choice of time constant. For the particular silicon drift detector (SDD)-EDS and time cons ...
314 20 20.2.4 Choosing the Beam Current After the analyst has chosen the EDS time constant, the detector solid angle (for a retr ...
315 20 . Fig. 20.3 SDD-EDS spectra of NIST SRM (glass K412, E 0 = 20 keV: a, b at 3 % dead-time (red); c 3 % (red) and 29 % dead ...
316 20 20.3 Examples of the k-ratio/Matrix Correction Protocol with DTSA II (Newbury and Ritchie 2015b) 20.3.1 Analysis of Major ...
317 20 choice of beam energy. If the beam energy can be decreased, considering also the constraints imposed by having sufficient ...
318 20 20.3.2 Analysis of Major Constituents (C > 0.1 Mass Fraction) with Severely Overlapping Peaks PbS The throughput and t ...
319 20 20.3.3 Analysis of a Minor Constituent with Peak Overlap From a Major Constituent The problem of accurately recovering pe ...
320 20 quantification suite of elements. A third iteration may be necessary to recover constituents present at the trace level n ...
321 20 3.0 0 1 000 2 000 3 000 4 000 0 5 000 10 000 15 000 20 000 a b 5 000 3.2 3.4 3.6 3.8 4.0 4.2 4.4 4.6 4.8 5.0 Photon energ ...
322 20 a24 000 22 000 20 000 18 000 16 000 14 000 12 000 10 000 8 000 6 000 4 000 2 000 0 3.0 3.5 4.0 4.5 5.0 Photon energy (keV ...
323 20 analysis (. Table 20.9), despite the severe interference from the Ti constituent which has a concentration more than four ...
324 20 composition to a particular unknown specimen. For many simple binary as well as more complex mixtures of elements, Nature ...
325 20 . Fig. 20.11 a Stainless steel, fitting for Si, Cr, Fe, Ni, and Mo; residual in blue. b Expanded vertical scale, note det ...
326 20 the results listed in. Table 20.11 (first analysis). The analyti- cal total is anomalously low at 0.7635. The second roun ...
327 20 a 350 000 b 300 000 250 000 200 000 150 000 100 000 50 000 0 0.0 1.0 2.0 3.0 4.0 5.0 Photon energy (keV) Counts 6.0 7.0 8 ...
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